Instrumental Chemical Analysis

 

 

FACULTY

ENGINEERING

DEPARTMENT

CHEMICAL ENGINEERING

LEVEL OF STUDY

UNDERGRADUATE

SEMESTER OF STUDY

3o

COURSE TITLE

Instrumental Chemical Analysis
COURSEWORK BREAKDOWNTEACHING WEEKLY HOURSECTS Credits
Lectures3
Laboratory2
Projects0

TOTAL

5
COURSE TYPE General Background
PREREQUISITES
LANGUAGE OF INSTRUCTION/EXAMSGreek
COURSE DELIVERED TO ERASMUS STUDENTSYes

MODULE WEB PAGE (URL)

https://eclass.uowm.gr/courses/CHEMENG170/


2. LEARNING OUTCOMES

Learning Outcomes

Upon successful completion of the module, students should acquire the following knowledge, abilities and skills:
• To know the basic principles, instrumentation and applications of chromatography.
• To know the basic principles, instrumentation and applications of spectroscopic techniques.
• He/She will be familiar with types of analytical methods, analytical instruments, instrumentation and methodology of calibration of instruments.
• He/She will be able to choose an instrumental method of analysis depending on the application and the analysis needs that he/she has to address.


General Skills

Search, analysis and synthesis of data and information, using the necessary technologies. Adapting to new situations. Decision-making. Autonomous work. Teamwork.


3. COURSE CONTENTS

Theory:
• Introduction to Instrumental Analysis
• Quantification Techniques
• Ultraviolet – Visible spectroscopy
• Flame Emission Spectroscopy
• Atomic Absorption Spectroscopy
• Mass Spectrometry
• Introduction to Chromatographic Analysis Techniques
• Gas Chromatography
• Paper Chromatography and Thin Layer Chromatography
• Ionic Chromatography
• Liquid Column Chromatography
Lab:
• Statistical Data Analysis
• Granulometric Analysis of Solids
• Conductivity
• Ion-exchange Chromatography
• Titration of Diprotic Acids
• Gas Chromatography
• Spectrophotometric Determination of Binary Mixtures
• Temperature Effect on Chemical Reaction Rate
• Ions Selective Electrodes
• Complexometric Determinations – Water Hardness
• FTIR – Infrared spectroscopy


4. TEACHING METHODS – ASSESSMENT

MODE OF DELIVERY
Face-to-Face
USE OF INFORMATION AND COMMUNICATION TECHNOLOGY
Use of ICT in teaching and communication with students

TEACHING METHODS
Method descriptionSemester Workload
Lectures39
Laboratory Exercises26
Study & analysis of literature39
Writing assignments26
Course Total
ASSESSMENT METHODS The total grade of the course is derived by 70% from the grade of the theory (written examination) and by 30% from the grade of the laboratory, which results from the grade of the Laboratory Assignments (LA), the grade of the Assessment Tests (AT), as well as the grade of the Final Examination (FE), and is given by the relationship:
0,25·(LA) + 0,25·(AT) + 0,5·(FE) = Final laboratory grade corresponding to 30% of the final grade.


5. RESOURCES

Suggested bibliography :

- Recommended Book Resources:
1. «Principles of Instrumental Analysis» Skoog, Holler, Nieman, Kostarakis Publishing (ISBN 978-960-87655-7-3)
2. «Modern Methods in Chemical Analysis», Pecsok, Shields, Cairns, McWilliam, Pnevmatikos Publishing (ISBN: 960-7258-27-4)-
3. «Instrumental Analysis» T. Hadjiioannou, M.A. Kouppari, University of Athens Publishing (ISBN: 960-220-750-7)
- Related Article/Paper Resources:
Relevant publications in peer reviewed international journals

Related academic journals: